3.1 Estancias en cooperación internacional
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PublicationVacancy ordered gamma-Fe2O3 nanoparticles functionalized with nanohydroxyapatite: XRD, FTIR, TEM, XPS and Mossbauer studies(Elsevier B.V., 2016)
;Guivar, JAR ;Sanches, EA ;Bruns, F ;Sadrollahi, E ;Morales, MA ;Lopez, EOLitterst, FJVacancy ordered maghemite (γ-Fe2O3) nanoparticles functionalized with nanohydroxyapatite (HAp – Ca10(PO4) 6(OH)2) have been successfully synthesized using an inexpensive co-precipitation chemical route. Evidence for the presence of vacancy order in maghemite was shown by the superstructure lines observed in X-ray diffraction. The adsorption of carboxyl groups of citric acid (C6H8O7) onto γ-Fe2O3 nanoparticles was investigated by FTIR, XPS and Mössbauer spectroscopy. -
PublicationVacancy ordered γ-Fe 2 O 3 nanoparticles functionalized with nanohydroxyapatite: XRD, FTIR, TEM, XPS and Mössbauer studies(Elsevier, 2016)
;Ramos Guivar J.A. ;Sanches E.A. ;Bruns F. ;Sadrollahi E. ;Morales M.A. ;López E.O.Litterst F.J.Vacancy ordered maghemite (γ-Fe2O3) nanoparticles functionalized with nanohydroxyapatite (HAp – Ca10(PO4) 6(OH)2) have been successfully synthesized using an inexpensive co-precipitation chemical route. Evidence for the presence of vacancy order in maghemite was shown by the superstructure lines observed in X-ray diffraction. The adsorption of carboxyl groups of citric acid (C6H8O7) onto γ-Fe2O3 nanoparticles was investigated by FTIR, XPS and Mössbauer spectroscopy. From XPS surface analysis, two binding energies related to oxygen were attributed to bindings between C6H8O7/γ- Fe2O3 and C6H8O7/HAp from an interfacial reaction promoted by strongly adsorbed H2O molecules at the surface of these nanomaterials.